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Visible-Light-Driven Neutral Nitrogen Radical Mediated Intermolecular Styrene Difunctionalization

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成果类型:
期刊论文
作者:
Zhao, Quan-Qing;Li, Man;Xue, Xiao-Song*;Chen, Jia-Rong*;Xiao, Wen-Jing*
通讯作者:
Chen, Jia-Rong;Xiao, Wen-Jing;Xue, Xiao-Song
作者机构:
[Zhao, Quan-Qing; Chen, Jia-Rong; Xiao, WJ; Xiao, Wen-Jing] Cent China Normal Univ, Hubei Int Sci & Technol Cooperat Base Pesticide &, Key Lab Pesticides & Chem Biol, CCNU uOttawa Joint Res Ctr,Minist Educ,Coll Chem, 152 Luoyu Rd, Wuhan 430079, Hubei, Peoples R China.
[Li, Man; Xue, Xiao-Song] Nankai Univ, Coll Chem, State Key Lab Elementoorgan Chem, Tianjin 300071, Peoples R China.
通讯机构:
[Chen, JR; Xiao, WJ] C
[Xue, Xiao-Song] N
Cent China Normal Univ, Hubei Int Sci & Technol Cooperat Base Pesticide &, Key Lab Pesticides & Chem Biol, CCNU uOttawa Joint Res Ctr,Minist Educ,Coll Chem, 152 Luoyu Rd, Wuhan 430079, Hubei, Peoples R China.
Nankai Univ, Coll Chem, State Key Lab Elementoorgan Chem, Tianjin 300071, Peoples R China.
语种:
英文
期刊:
Organic Letters
ISSN:
1523-7060
年:
2019
卷:
21
期:
10
页码:
3861-3865
基金类别:
NNSFCNational Natural Science Foundation of China (NSFC) [91856119, 21622201, 21820102003, 21772053]; Science and Technology Department of Hubei Province [2016CFA050, 2017AHB047]; Program of Introducing Talents of Discipline to Universities of China (111 Program) [B17019]
机构署名:
本校为第一且通讯机构
院系归属:
化学学院
摘要:
A neutral nitrogen radical-mediation strategy, wherein the existing N-H moiety of substrates serves as a neutral nitrogen radical precursor to enable room-temperature intermolecular radical difunctionalization of styrenes under photoredox catalysis, is reported. The reaction shows high functional group tolerance and substrate scope with respect to both components, giving the corresponding products with generally good yields. Preliminary control experiments and DFT c...

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