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Generalized preparation of porous nanocrystalline zoned2O 4 superstructures from zinc ferrioxalate precursor and its superparamagnetic property

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成果类型:
期刊论文
作者:
Wang, Man;Ai, Zhihui*;Zhang, Lizhi
通讯作者:
Ai, Zhihui
作者机构:
[Zhang, Lizhi; Wang, Man; Ai, Zhihui] Cent China Normal Univ, Coll Chem, Key Lab Pesticide & Chem Biol, Minist Educ, Wuhan 430079, Peoples R China.
通讯机构:
[Ai, Zhihui] C
Cent China Normal Univ, Coll Chem, Key Lab Pesticide & Chem Biol, Minist Educ, Wuhan 430079, Peoples R China.
语种:
英文
期刊:
Journal of Physical Chemistry C
ISSN:
1932-7447
年:
2008
卷:
112
期:
34
页码:
13163-13170
基金类别:
National Basic Research Program of China [2007CB613301]; National Science Foundation of China [20503009, 20673041, 20777026]; Program for New Century Excellent Talents in University [NCET-07-0352]; Ministry of Education of China [108097]; Postdoctors Foundation of China [20070410935]
机构署名:
本校为第一且通讯机构
院系归属:
化学学院
摘要:
In this paper, porous nanocrystalline ZnFe2O4 “timber-like” superstructures were synthesized through the thermal decomposition of zinc ferrioxalate precursor prepared from metal sulfates and sodium oxalate without adding any additives. The resulting ZnFe2O4 superstructures were systematically characterized by X-ray powder diffraction (XRD), thermogravimetry and differential scanning calorimetry (TG-DSC), scanning electronic microscopy (SEM), transmission electron microscopy (TEM) and high-resolution TEM (HRTEM), X-ray photoelectron spectrosco...

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