Transition-metal-free synthesis of 1,4-benzoxazepines via [4+3]-cycloaddition of para-quinone methides with azaoxyallyl cations

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期刊论文

作者：

Zhou, Shuang-Jing;Cheng, Xiao;Hu, Chun-Xia;Xu, Guo-Yong;Xiao, Wen-Jing*;...

通讯作者：

Xuan, Jun;Xiao, Wen-Jing

作者机构：

[Zhou, Shuang-Jing; Cheng, Xiao; Hu, Chun-Xia; Xuan, Jun] Anhui Univ, Coll Chem & Chem Engn, Anhui Prov Key Lab Chem Inorgan Organ Hybrid Func, Hefei 230601, Peoples R China.

[Zhou, Shuang-Jing; Cheng, Xiao; Hu, Chun-Xia; Xuan, Jun] Anhui Univ, Coll Chem & Chem Engn, Key Lab Funct Inorgan Mat Anhui Prov, Hefei 230601, Peoples R China.

[Xuan, Jun] Anhui Univ, Key Lab Struct & Funct Regulat Hybrid Mat, Minist Educ, Hefei 230601, Peoples R China.

[Xiao, Wen-Jing] Cent China Normal Univ, Coll Chem, Key Lab Pesticide & Chem Biol, Minist Educ, Wuhan 430079, Peoples R China.

[Xu, Guo-Yong] Anhui Univ, Inst Phys Sci & Informat Technol, Hefei 230601, Peoples R China.

通讯机构：

[Xuan, Jun] A

[Xiao, Wen-Jing] C

Anhui Univ, Coll Chem & Chem Engn, Anhui Prov Key Lab Chem Inorgan Organ Hybrid Func, Hefei 230601, Peoples R China.

Anhui Univ, Coll Chem & Chem Engn, Key Lab Funct Inorgan Mat Anhui Prov, Hefei 230601, Peoples R China.

Anhui Univ, Key Lab Struct & Funct Regulat Hybrid Mat, Minist Educ, Hefei 230601, Peoples R China.

语种：

英文

关键词：

4-benzoxazepines;para-quinone methides;azaoxyallyl cations;cycloaddition;transition-metal-free

期刊：

中国科学：化学英文版

ISSN：

1674-7291

年：

2021

卷：

期：

页码：

61-65

DOI：

10.1007/s11426-020-9832-9

基金类别：

supported by the National Natural Science Foundation of China （21971001, 21702001）； the Natural Science Foundation of Anhui Province （1808085MB47）； the Open Fund for Discipline Construction;Institute of Physical Science and Information Technology； Anhui University and the Start-up Grant from Anhui University；

机构署名：

本校为通讯机构

院系归属：

化学学院

摘要：

A formal [4+3]-cycloaddition reaction of ortho-hydroxyphenyl-substituted para-quinone methides (p-QMs) with in-situ generated azaoxyallyl cations is reported. The reaction occurs under very mild reaction conditions (transition-metal free, room temperature, cheap inorganic base) and provides a very efficient route to a series of biologically important 1,4-benz...

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Transition-metal-free synthesis of 1,4-benzoxazepines via [4+3]-cycloaddition of para-quinone methides with azaoxyallyl cations

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