I-2/PhI(OAc)(2) Copromoted Amination Reaction: Synthesis of alpha-Dicarbonylsulfoximine Derivatives by Incorporating an Intact Dimethyl Sulfoxide

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成果类型：

期刊论文

作者：

Zhao, Peng;Wu, Xia;Geng, Xiao;Wang, Can;Zhou, You;...

通讯作者：

Wu, An-Xin

作者机构：

[Zhao, Peng; Wu, Xia; Geng, Xiao; Wang, Can; Zhou, You; Wu, Yan-Dong; Wu, An-Xin] Cent China Normal Univ, Key Lab Pesticide & Chem Biol, Minist Educ, Coll Chem, Wuhan 430079, Hubei, Peoples R China

通讯机构：

[Wu, An-Xin] C

Cent China Normal Univ, Key Lab Pesticide & Chem Biol, Minist Educ, Coll Chem, Wuhan 430079, Hubei, Peoples R China.

语种：

英文

期刊：

JOURNAL OF ORGANIC CHEMISTRY

ISSN：

0022-3263

年：

2019

卷：

期：

页码：

8322-8329

DOI：

10.1021/acs.joc.9b01160

基金类别：

National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [21472056, 21602070, 21772051]; Fundamental Research Funds for the Central UniversitiesFundamental Research Funds for the Central Universities [CCNUI5ZX002, CCNU18QN011]; 111 ProjectMinistry of Education, China - 111 Project [B17019]

机构署名：

本校为第一且通讯机构

院系归属：

化学学院

摘要：

An I-2/PhI(OAc)(2) copromoted strategy using dimethyl sulfoxide as an "S/C2/O" source for preparing alpha-dicarbonylsulfoximine derivatives is reported. This process involves oxidative coupling to construct a C-N bond and electrophilic amination of dimethyl sulfoxide to afford an N = S bond, with dimethyl sulfoxide present in the final product as an intact molecule. Furthermore, tetramethylene sulfoxide as a solven...

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I-2/PhI(OAc)(2) Copromoted Amination Reaction: Synthesis of alpha-Dicarbonylsulfoximine Derivatives by Incorporating an Intact Dimethyl Sulfoxide

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