Remote Selective C−H Halogenation of Arylphosphine Oxides with Ferric Halides

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成果类型：

期刊论文

作者：

Yu, Hong;Lin, Xiuhua;Xu, Guang;Yin, Tingrui;Zhang, Ying;...

通讯作者：

Yu, GA;Dang, L;Yuan, J

作者机构：

[Xu, Guang; Chen, Jian; Yu, Hong; Liu, Jinpeng; Yin, Tingrui; Meng, Sixuan; Zhang, Ying; Yu, Guang-Ao] Cent China Normal Univ, Coll Chem, Int Joint Res Ctr Intelligent Biosensor Technol &, Natl Key Lab Green Pesticide, Wuhan 430079, Peoples R China.

[Lin, Xiuhua; Dang, Li; Dang, L] Shantou Univ, Dept Chem, Shantou 515063, Guangdong, Peoples R China.

[Lin, Xiuhua; Dang, Li; Dang, L] Shantou Univ, Key Lab Preparat & Applicat Ordered Struct Mat Gua, Shantou 515063, Guangdong, Peoples R China.

[Lin, Xiuhua; Dang, Li; Dang, L] Chem & Chem Engn Guangdong Lab, Shantou 515063, Guangdong, Peoples R China.

[Yuan, Jia; Yuan, J] Wuhan Text Univ, State Key Lab New Text Mat & Adv Proc Technol, Wuhan 430200, Peoples R China.

通讯机构：

[Yuan, J ] W

[Yu, GA ] C

[Dang, L ] S

Cent China Normal Univ, Coll Chem, Int Joint Res Ctr Intelligent Biosensor Technol &, Natl Key Lab Green Pesticide, Wuhan 430079, Peoples R China.

Shantou Univ, Dept Chem, Shantou 515063, Guangdong, Peoples R China.

语种：

英文

关键词：

Aryl phosphine oxides;Bromination;Chlorination;Ferric halides;C−H activation

期刊：

ADVANCED SYNTHESIS & CATALYSIS

ISSN：

1615-4150

年：

2023

卷：

365

期：

页码：

3101-3106

DOI：

10.1002/adsc.202300486

基金类别：

National Natural Science Foundation of China [21472060, 21772058, 21072071]; 111 Project [B17019]; self-determined research funds of CCNU from the colleges' basic research and operation of MOE [CCNU17CG0011, CCNU17KYZHSY07, CCNU18KYZHSY06]

机构署名：

本校为第一且通讯机构

院系归属：

化学学院

摘要：

We developed the remote selective C-H bromination for the synthesis of C4 & PRIME;-brominated biarylphosphine oxides using FeBr3 as a brominating reagent. C3 & PRIME;-Brominated products were obtained in reactions with substrates bearing a 2,4,6-triisopropyl substituent on the bottom ring. Moreover, direct access to C5-chlorinated peri-substituted(1-naphthalenyl)phosphines is developed using FeCl3 as a chlorinating reagent. These halogenated compounds can be utilized for cross-coup...

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Remote Selective C−H Halogenation of Arylphosphine Oxides with Ferric Halides

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