WS: floriated nanocrystals were prepared by solid - gas reaction with tungsten oxide powder and H2S gas on substrate of anodic aluminum oxide (AAO) template. The microstruture of the WS2 floriated nanocrystal was investigated by means of transmission electron microscopy (TEM), X-ray diffraction (XRD) and scanning electron microscopy (SEM). The thickness of every petal is about 30nm, length and width of the WS2 layered monocrystal are several microns respectively. The influencing conditions of WS2 floriated na...