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3-(4-Chloro-phen-yl)-2-(2,4-dichloro-phen-oxy)-5-methyl-8,9,10, 11-tetra-hydro-2-benzothieno[2′,3′:2,3]pyrido[4,5-d]pyrimidin-4(3H) -one dichloro-methane solvate

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成果类型:
期刊论文
作者:
Liu, Jian-Chao*
通讯作者:
Liu, Jian-Chao
作者机构:
[Liu, Jian-Chao; Liu, JC] Cent S Univ, Coll Chem & Chem Engn, Changsha 410083, Peoples R China.
[Liu, JC] Cent China Normal Univ, Dept Journalism, Wuhan 430
通讯机构:
[Liu, Jian-Chao] C
Cent S Univ, Coll Chem & Chem Engn, Changsha 410083, Peoples R China.
语种:
英文
期刊:
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY
ISSN:
2053-2296
年:
2007
卷:
63
期:
12
页码:
o4571-o4571
机构署名:
本校为其他机构
院系归属:
新闻传播学院
摘要:
In the structure of the title compound, C26H18Cl3N3O2S·CH2Cl2, the C - S bond lengths in the thio-phene ring [1.733 (5) and 1.735 (5) Å] are equivalent and long compared with the values observed in both free thio-phene, measured using electron diffraction, and thieno[2,3-c]pyridine. The central thienopyridine ring system is planar. The pyrimidinone ring forms a dihedral angle of 3.1 (2)° with the pyridine ring. The chloro- and dichloro-phenyl rings form dihedral angles of 75.2 (2) and 85.5 (2)°, respectively, with the pyrimidinone ring. The...

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