Asymmetric [3+2] Photocycloaddition of & beta;-Keto Esters and Vinyl Azides by Dual Photoredox/Nickel Catalysis

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成果类型：

期刊论文

作者：

Zhou, Xue-Song;Zhang, Zhihan;Qu, Wen-Yuan;Liu, Xiao-Peng;Xiao, Wen-Jing*;...

通讯作者：

Xiao, Wen-Jing;Chen, JR;Jiang, M;Xiao, WJ

作者机构：

[Qu, Wen-Yuan; Xiao, Wen-Jing; Chen, Jia-Rong; Zhou, Xue-Song; Liu, Xiao-Peng; Xiao, WJ; Zhang, Zhihan; Chen, JR] Cent China Normal Univ, Coll Chem, Wuhan 430079, Hubei, Peoples R China.

[Jiang, Min] Hangzhou Normal Univ, Coll Mat Chem & Chem Engn, Hangzhou 310036, Zhejiang, Peoples R China.

[Xiao, Wen-Jing; Chen, Jia-Rong; Xiao, WJ; Chen, JR] Wuhan Inst Photochem & Technol, Wuhan 430083, Hubei, Peoples R China.

[Xiao, Wen-Jing; Xiao, WJ] Shanghai Inst Organ Chem, State Key Lab Organometall Chem, Shanghai 200032, Peoples R China.

[Chen, Jia-Rong; Chen, JR] Henan Normal Univ, Sch Chem & Chem Engn, Xinxiang 453007, Peoples R China.

通讯机构：

[Jiang, M ] H

[Xiao, WJ ] S

[Xiao, WJ; Chen, JR ] C

Cent China Normal Univ, Coll Chem, Wuhan 430079, Hubei, Peoples R China.

Hangzhou Normal Univ, Coll Mat Chem & Chem Engn, Hangzhou 310036, Zhejiang, Peoples R China.

语种：

英文

期刊：

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY

ISSN：

0002-7863

年：

2023

卷：

145

期：

页码：

12233-12243

DOI：

10.1021/jacs.3c02485

基金类别：

National Natural Science Foundation of China [21971081, 22171099, 21820102003, 91956201, 22203034, 92256301]; Nation Key Ramp;D Program of China [2022YFA1506100]; Zhejiang Natural Science Foundation [LQ20B020010]; Open Research Fund of School of Chemistry and Chemical Engineering, Henan Normal University [2021YB02]; Double-Thousand Talents Plan of Jiangxi Province; Knowledge Innovation Program of Wuhan-Basic Research; Program of Introducing Talents of Discipline to Universities of China (111 Program); [2022013301015173]; [B17019]

机构署名：

本校为第一且通讯机构

院系归属：

化学学院

摘要：

Photocatalytic [3 + 2] cycloadditions and control of stereochemistry have remained a substantial challenge, particularly in the context of heterocycle synthesis; sporadic successful examples have involved enantioselective [3 + 2] photocycloaddition between redox-active direct group-containing cyclopropanes and alkenes for creation of cyclopentanes. Herein, we report a cooperative catalytic system comprising a chiral nickel Lewis acid catalyst and an organic photocatalyst fueled by visible-light irradiation that allows for the hitherto elusive a...

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Asymmetric [3+2] Photocycloaddition of & beta;-Keto Esters and Vinyl Azides by Dual Photoredox/Nickel Catalysis

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