Novel ultra-fine NiO/SnO2 nano-particles (NPs) have been fabricated by creatively using carbon black (CB) as a frame and dispersing agent and applied as gas-sensing materials. In a typical synthesis, a precursor composed of mixed NiO/SnO2 NPs and CB was initially prepared. Subsequently, the ultra-fine NiO/SnO2 NPs were obtained by a thermal treatment of the precursor. The final products were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, scanning electron microscopy, transmission electron microscopy, and Brunauer Emmett T...