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Determination of four sulfonylurea herbicides in tea by matrix solid-phase dispersion cleanup followed by dispersive liquid-liquid microextraction

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成果类型:
期刊论文
作者:
Liang, Pei*;Wang, Jinjin;Liu, Guojiao;Guan, Jinyan
通讯作者:
Liang, Pei
作者机构:
[Liu, Guojiao; Guan, Jinyan; Wang, Jinjin; Liang, Pei] Cent China Normal Univ, Key Lab Pesticide & Chem Biol, Minist Educ, Coll Chem, Wuhan 430079, Hubei, Peoples R China.
通讯机构:
[Liang, Pei] C
Cent China Normal Univ, Key Lab Pesticide & Chem Biol, Minist Educ, Coll Chem, Wuhan 430079, Hubei, Peoples R China.
语种:
英文
关键词:
Dispersive liquid-liquid microextraction;High-performance liquid chromatography;Matrix solid-phase dispersion;Sulfonylurea herbicides;Tea samples
期刊:
JOURNAL OF SEPARATION SCIENCE
ISSN:
1615-9306
年:
2014
卷:
37
期:
17
页码:
2380-2387
机构署名:
本校为第一且通讯机构
院系归属:
化学学院
摘要:
Matrix solid-phase dispersion combined with dispersive liquid-liquid microextraction has been developed as a new sample pretreatment method for the determination of four sulfonylurea herbicides (chlorsulfuron, bensulfuron-methyl, chlorimuron-ethyl, and pyrazosulfuron) in tea by high-performance liquid chromatography with diode array detection. The extraction and cleanup by matrix solid-phase dispersion was carried out by using CN-silica as dispersant and carbon nanotubes as cleanup sorbent eluted with acidified dichloromethane. The eluent of matrix solid-phase dispersion was evaporated and red...

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