Copper-catalyzed thiocyanation of cyclobutanone oxime esters using ammonium thiocyanate

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成果类型：

期刊论文

作者：

Zhao, Xia;Sun, Tengteng;Gu, Wenxin;Qin, Jingwen;Lu, Kui;...

通讯作者：

Zhao, X;Ye, F

作者机构：

[Zhao, Xia; Gu, Wenxin; Sun, Tengteng; Qin, Jingwen] Tianjin Normal Univ, Tianjin Key Lab Struct & Performance Funct Mol, Key Lab Inorgan Organ Hybrid Funct Mat Chem, Minist Educ,Coll Chem, Tianjin 300387, Peoples R China.

[Ye, Fei] Cent China Normal Univ, CCNU uOttawa Joint Res Ctr, Key Lab Pesticides & Chem Biol, Minist Educ,Coll Chem, Wuhan 430079, Peoples R China.

[Lu, Kui] Tianjin Univ Sci & Technol, Coll Biotechnol, China Int Sci & Technol Cooperat Base Food Nutr Sa, Tianjin 300457, Peoples R China.

通讯机构：

[Zhao, X ] T

[Ye, F ] C

Tianjin Normal Univ, Tianjin Key Lab Struct & Performance Funct Mol, Key Lab Inorgan Organ Hybrid Funct Mat Chem, Minist Educ,Coll Chem, Tianjin 300387, Peoples R China.

Cent China Normal Univ, CCNU uOttawa Joint Res Ctr, Key Lab Pesticides & Chem Biol, Minist Educ,Coll Chem, Wuhan 430079, Peoples R China.

语种：

英文

期刊：

Organic & Biomolecular Chemistry

ISSN：

1477-0520

年：

2024

卷：

期：

页码：

1466-1474

DOI：

10.1039/d3ob01898a

基金类别：

National Natural Science Foundation of China [22277089, 22077095]; National Natural Science Foundation of China

机构署名：

本校为通讯机构

院系归属：

化学学院

摘要：

A copper-catalyzed thiocyanation of cycloketone oxime esters with ammonium thiocyanate has been developed for the first time. This innovative approach allows access to cyano and thiocyano bifunctionally substituted alkanes, which can be further transformed into their respective trifluoromethylthiol-substituted or difluoromethylthiol-substituted alkylnitriles, alkynyl sulfides, and phosphorothioate esters. The readily available nature of ammonium thiocyanate and the cost-effectiveness of the copper catalyst make this method a pr...

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Copper-catalyzed thiocyanation of cyclobutanone oxime esters using ammonium thiocyanate

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