Thirteen new 2-aryloxy-3-(4-fluorophenyl)-3,5,6,7-tetrahydro-4H- cyclopenta[4,5]thieno[2,3-d]-pyrimidin-4-ones were synthesized in 58%~73% yields by aza-Wittig reaction of (4,5,6-trihydrocyclopentathiophen-2-ylimino) (triphenyl)phosphorane with 4-fluorophenyl iso-cyanate, and subsequent reaction with phenols. Their structures were confirmed by IR, 1H NMR, MS techniques and elemental analyses. Their bacteriostatic activities were tested and the results showed that their bacteriostatic activities against fungus (Penicill...