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Diethyl 2,6-bis-(4-ethynylphen-yl)-4,8-dioxoperhydro-2,3a,4a,6,7a,8a-hexa- aza-cyclo-penta-[def]fluorene-8b,8c-dicarboxyl-ate

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成果类型:
期刊论文
作者:
Hu, Sheng-Li*;Wang, Shuai;Cao, Liping
通讯作者:
Hu, Sheng-Li
作者机构:
[Cao, Liping; Hu, Sheng-Li; Wang, Shuai] Cent China Normal Univ, Coll Med, Minist Educ, Key Lab Pest & Chem Biol, Wuhan 430079, Peoples R China.
通讯机构:
[Hu, Sheng-Li] C
Cent China Normal Univ, Coll Med, Minist Educ, Key Lab Pest & Chem Biol, Wuhan 430079, Peoples R China.
语种:
英文
期刊:
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY
ISSN:
2053-2296
年:
2007
卷:
63
期:
12
页码:
O4542-U3520
机构署名:
本校为第一且通讯机构
院系归属:
化学学院
摘要:
The mol-ecule of the title compound, C30H28N6O6, a glycoluril derivative, lies on a twofold rotation axis with two ethyl acetate groups bonded to the convex face of the glycoluril system. The dihedral angle between the imidazolone rings is 73.12 (3)°. Two symmetry-equivalent six-membered triazine rings are fused to the glycouril unit to form rigid side walls of a mol-ecular clip. The crystal structure is stabilized by weak inter-molecular C - H⋯O hydrogen bonds. The ethyl ester group is disordered over two sites of occupancy 0.5...

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