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Synthesis and Structure of 5-Amino-6-(4-fluorophenylamino)-3-methylthio-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one

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成果类型:
期刊论文
作者:
Wang Hong-Qing*;Zhou Wei-Ping;Liu Zhao-Jie
通讯作者:
Wang Hong-Qing
作者机构:
[Wang Hong-Qing] Nanhua Univ, Coll Chem & Chem Engn, Hengyang 421001, Peoples R China.
Cent China Normal Univ, Coll Chem, Wuhan 430079, Peoples R China.
Minist Agr, Key Lab Pesticide Chem & Applicat Technol, Beijing 100094, Peoples R China.
通讯机构:
[Wang Hong-Qing] N
Nanhua Univ, Coll Chem & Chem Engn, Hengyang 421001, Peoples R China.
语种:
英文
关键词:
1,5-dihydroe;synthesis;crystal structure
期刊:
Chinese Journal of Structural Chemistry
ISSN:
0254-5861
年:
2006
卷:
25
期:
9
页码:
1105-1109
基金类别:
Project supported by the Natural Science Foundation of Hunan Province (No. 05JJ30022) and Key Laboratory of Pesticide Chemistry & Application Technology, Ministry of Agriculture, China (No. PCAT200401);
机构署名:
本校为其他机构
院系归属:
化学学院
摘要:
The title compound (C18H15FN6OS) has been synthesized and its crystal structure was determined by X-ray analysis. The crystal belongs to monoclinic system, space group P21/n with a = 13.983(10), b = 7.337(5), c = 16.702(12) (A), α = 90, β = 98.277(12), γ = 90°, V = 1696(2)(A)3, Z = 4, Dc= 1.498 g/cm3, Mr = 382.42,μ = 0.224 mm-1, F(000) = 792, the final R = 0.0362 and wR = 0.0878 for 2579 observed reflections with I > 2σ(Ⅰ). In the title compound, the atoms of C(1),C(2), C(3), C(4), C(5), N(1), N(2), N(3), N(4), N(5), N(6), O(1) and S(1)...

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