期刊论文

Peng Hao

英文

Chinese Journal of Structural Chemistry

0254-5861

2011

30

12

1765-1769

10.14102/j.cnki.0254-5861.2011.12.022

National Basic Research Program of ChinaNational Basic Research Program of China [2010CB126100]; National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [21002037, 20772042]; PCSIRTProgram for Changjiang Scholars & Innovative Research Team in University (PCSIRT) [IRT0953]

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A new crystal of N,N-bis(4-nitrophenylcarbamothioyl)isophthalamide DMF solva- te has been prepared at room temperature and characterized by elemental analysis and IR, MS, ~1H NMR spectra and X-ray single-crystal determination. The complex crystallizes in monoclinic, space group P2_1/c with a = 11.2093(12), b = 22.081(2), c = 13.9640(15) A,,,,= 112.128(2)°,1V = 3201.8(6) A~3, C_(28)H_(30)N_8O_8S_2, M_r = 670.72, Dc = 1.391 Mg/m~3, Z = 4,,,= 0.228 mm~(-1), F(000) = 1400, the final R = 0.0483 and wR = 0.1411 (I > 2>(I)). The molecular ...