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Synthesis, Characterization and X-ray Crystal Structure of O,Oˊ-Dipropyl α-(2,4-Dichlorolphenoxyacylamido)-α-(4-methoxyphenyl) Methylphosphonates

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成果类型:
期刊论文
作者:
宁丽红;彭浩;贺红武
通讯作者:
He, H.-W.
作者机构:
Key Laboratory of Pesticide and Chemical Biology, Ministry of Education and College of Chemistry, Central China Normal University, Wuhan 430079, China
College of Science, Huazhong Agricultural University, Wuhan 430070, China
通讯机构:
Key Laboratory of Pesticide and Chemical Biology, Ministry of Education and College of Chemistry, Central China Normal University, China
语种:
英文
关键词:
Phosphonate;X-ray crystallography
关键词(中文):
甲基膦酸酯;甲氧基苯基;晶体结构;X-射线;丙基;合成;表征;核磁共振谱
期刊:
Chinese Journal of Structural Chemistry
ISSN:
0254-5861
年:
2013
卷:
32
期:
9
页码:
1392-1396
基金类别:
supported by the National Basic Research Program of China(2010CB126100);
机构署名:
本校为第一且通讯机构
院系归属:
化学学院
摘要:
A new crystal of O,Oˊ-dipropyl-α-(2,4-dichlorolphenoxyacylamido)-α-(4-methoxyphenyl) methylphosphonates has been prepared at room temperature and characterized by elemental analysis and IR,MS,1H NMR spectra,13C NMR spectra and X-ray single-crystal determination.The complex crystallizes in triclinic,space group P1 with a = 7.858(2),b = 12.621(4),c = 12.621(4),α = 96.17(3),β = 90.960(3),γ = 90.960(3)°,V = 1243.9(7)3,Dc = 1.346 Mg/m3,Z ...

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