期刊论文

Peng Hao

英文

Chinese Journal of Structural Chemistry

0254-5861

2014

33

2

223-227

10.14102/j.cnki.0254-5861.2014.02.009

National Basic Research Program of ChinaNational Basic Research Program of China [2010CB126100]; National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [21002037, 21172090]; PCSIRTProgram for Changjiang Scholars & Innovative Research Team in University (PCSIRT) [IRT0953]

本校为第一且通讯机构

A new crystal of 4-fluoro-N-(2-methyl-5-((2-(p-tolyloxy)acetamido)methyl)pyrimidin-4-yl)benzamide has been prepared at room temperature and characterized by ~1H NMR, ~(13)CNMR, IR, MS, elemental analysis and X-ray single-crystal determination. The compound crystallizes in monoclinic, space group P2_1/c with a = 17.226(5), b = 13.934(4), c = 17.262(5) A, b = 92.180(5)°, V = 4140(2) A~3, D_c = 1.311 g/cm~3, Z = 8, F(000) = 1712 and m = 0.095 mm~(-1). The molecular packin...