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Asymmetric Deoxygenative Cyanation of Benzyl Alcohols Enabled by Synergistic Photoredox and Copper Catalysis

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成果类型:
期刊论文
作者:
Chen, Hong-Wei;Lu, Fu-Dong;Cheng, Ying*;Jia, Yue;Lu, Liang-Qiu*;...
通讯作者:
Cheng, Ying;Lu, Liang-Qiu
作者机构:
[Lu, Fu-Dong; Lu, Liang-Qiu; Cheng, Ying; Jia, Yue; Xiao, Wen-Jing; Chen, Hong-Wei; Lu, LQ] Cent China Normal Univ, Coll Chem, CCNU uOttawa Joint Res Ctr, Minist Educ,Key Lab Pesticide & Chem Biol, 152 Luoyu Rd, Wuhan 430079, Hubei, Peoples R China.
[Xiao, Wen-Jing] Shanghai Inst Organ Chem, State Key Lab Organometall Chem, 345 Lingling Rd, Shanghai 200032, Peoples R China.
通讯机构:
[Cheng, Y; Lu, LQ] C
Cent China Normal Univ, Coll Chem, CCNU uOttawa Joint Res Ctr, Minist Educ,Key Lab Pesticide & Chem Biol, 152 Luoyu Rd, Wuhan 430079, Hubei, Peoples R China.
语种:
英文
关键词:
Deoxygenative cyanation;Synergistic catalysis;Photocatalysis;Enantioselectivity;Chiral nitrile
期刊:
中国化学
ISSN:
1001-604X
年:
2020
卷:
38
期:
12
页码:
1671-1675
基金类别:
National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [21901080, 21822103, 21820102003, 91956201]; Program of Introducing Talents of Discipline to Universities of China (111 Program) [B17019]; Natural Science Foundation of Hubei ProvinceNatural Science Foundation of Hubei Province [2017AHB047]; International Joint Research Center for Intelligent Biosensing Technology and Health
机构署名:
本校为第一且通讯机构
院系归属:
化学学院
摘要:
. Summary of main observation and conclusion: An enantioselective deoxygenative cyanation of benzyl alcohols was accomplished for the first time through the synergistic photoredox and copper catalysis. This reaction features the use of organic photosensitizer and low-cost 3d metal catalyst, simple and safe operations, and extremely mild conditions. A variety of chiral benzyl nitriles were produced in generally good yields and high level of enantiocontrols from readily ava...

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