Visible-Light-Driven Four-Component Radical Relay Aminocarbonylation of Unactivated Alkenes

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成果类型：

期刊论文

作者：

Lu, Bin;Bao, Feng-Shuo;He, Zi-Wei;Xiao, Wen-Jing;Chen, Jia-Rong

通讯作者：

Chen, JR

作者机构：

[Lu, Bin; Bao, Feng-Shuo; Xiao, Wen-Jing; Chen, Jia-Rong; He, Zi-Wei; Chen, JR] Cent China Normal Univ, Coll Chem, Engn Res Ctr Photoenergy Utilizat Pollut Control &, 152 Luoyu Rd, Wuhan 430079, Hubei, Peoples R China.

[Xiao, Wen-Jing; Chen, Jia-Rong; Chen, JR] Wuhan Inst Photochem & Technol, 7 North Bingang Rd, Wuhan 430083, Hubei, Peoples R China.

[Chen, Jia-Rong; Chen, JR] Gannan Normal Univ, Key Lab Organopharmaceut Chem Jiangxi Prov, Ganzhou 341000, Jiangxi, Peoples R China.

通讯机构：

[Chen, JR ] C

Cent China Normal Univ, Coll Chem, Engn Res Ctr Photoenergy Utilizat Pollut Control &, 152 Luoyu Rd, Wuhan 430079, Hubei, Peoples R China.

Wuhan Inst Photochem & Technol, 7 North Bingang Rd, Wuhan 430083, Hubei, Peoples R China.

Gannan Normal Univ, Key Lab Organopharmaceut Chem Jiangxi Prov, Ganzhou 341000, Jiangxi, Peoples R China.

语种：

英文

关键词：

Visible light;Photoredox catalysis;Radical aminocarbonylation;Multicomponent reaction;Carbon monoxide;Unactivated alkenes;Amides;Reaction mechanisms

期刊：

中国化学

ISSN：

1001-604X

年：

2024

卷：

期：

页码：

990-996

DOI：

10.1002/cjoc.202300733

基金类别：

National Natural Science Foundation of China; Double-Thousand Talents Plan of Jiangxi Province [jxsq2023102004]; Open Research Fund of School of Chemistry and Chemical Engineering, Henan Normal University [2021YB02]; Program of Introducing Talents of Discipline to Universities of China [B17019]; [21971081]; [22171099]; [21820102003]; [91956201]; [22203034]; [92256301]

机构署名：

本校为第一且通讯机构

院系归属：

化学学院

摘要：

A visible‐light‐driven four‐component radical relay aminocarbonylation reaction of unactivated alkenes using 4CzIPN as an organic photocatalyst is developed, providing robust access to β‐fluoroalkyl amides with good yields and selectivity under metal‐free conditions. Importantly, this strategy also shows good compatibility with tertiary carbon radicals. Comprehensive Summary Catalytic four‐component radical carbonylation of unactivated alkenes has recently been recognized as a robust protocol for rapid construction of various structurall...

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Visible-Light-Driven Four-Component Radical Relay Aminocarbonylation of Unactivated Alkenes

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