Efficient selective formation of C - C single bonds and C = C double bonds by NBS-promoted oxidative coupling of beta-keto esters
作者：
Wang, Zhiguo
* ;Yin, Guodong;Chen, Aihua;Hu, Shengli;Wu, Anxin
（ 期刊：
Synthetic Communications ,2007年37(24):4399-4405 ISSN：0039-7911
通讯作者：
Wang, Zhiguo
作者机构：
[Wu, Anxin; Yin, Guodong; Wang, Zhiguo; Chen, Aihua; Hu, Shengli] Cent China Normal Univ, Coll Chem, Minist Educ, Key Lab Pesticide & Chem Biol, Wuhan 430079, Peoples R China.
通讯机构：
[Wang, Zhiguo] C;Cent China Normal Univ, Coll Chem, Minist Educ, Key Lab Pesticide & Chem Biol, Wuhan 430079, Peoples R China.
关键词：
active methylene groups;beta-keto esters;NBS;oxidative coupling;MOLECULAR-STRUCTURE;ATOM TRANSFER;CRYSTAL;TETRAACETYLETHANE;DICARBONYLS;CONSTANTS
摘要：
A new application of NBS, which results in the oxidative coupling of beta-keto esters to selectively form C - C single and C = C double bonds, can be controlled by the amount of NBS and t-BuOK employed. This methodology adds a new entry to C - C single and C = C double-bond formation between active methylene groups under mild conditions with high selectivity.
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Chiral molecular clips control orthogonal crystalline organization
作者：
Chen, Yunfeng
* ;She, Nengfang
（ ;Meng, Xianggao;Yin, Guodong;Wu, Anxin
（ ;...
期刊：
Organic Letters ,2007年9(10):1899-1902 ISSN：1523-7060
作者机构：
[Chen, Yunfeng] Cent China Normal Univ, Key Lab Pesticide & Chem Biol, Minist Educ, Coll Chem, Wuhan 430079, Peoples R China.;Univ Maryland, Dept Chem & Biochem, College Pk, MD 20742 USA.
通讯机构：
[Chen, Yunfeng] C;Cent China Normal Univ, Key Lab Pesticide & Chem Biol, Minist Educ, Coll Chem, Wuhan 430079, Peoples R China.
摘要：
Chiral molecular clips constitute a robust system for crystal engineering studies and undergo several levels of orthogonal organization including heterochiral dimerization, H-bond or metal-ligand mediated tape formation, and longitudinal packing of the tapes.
语种：
英文
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Toposelective synthesis under thermodynamic control and bioactivities of topoisomers based on diethoxycarbonyl glycoluril derivatives
作者：
Baohan Zhou;Guodong Yin;Zhiguo Wang;Yunfeng Chen;Anxin Wu
（ ;...
期刊：
科学通报(英文版) ,2006年51(17):2164-2168 ISSN：2095-9273
通讯作者：
Wu Anxin
作者机构：
[Anxin Wu; Zhiguo Wang; Guodong Yin; Wu Anxin; Yunfeng Chen; Jian Wan; Baohan Zhou] Cent China Normal Univ, Minist Educ, Dept Chem, Key Lab Pesticide & Chem Biol, Wuhan 430079, Peoples R China.
通讯机构：
[Wu Anxin] C;Cent China Normal Univ, Minist Educ, Dept Chem, Key Lab Pesticide & Chem Biol, Wuhan 430079, Peoples R China.
关键词：
biological activity;thermodynamic control;topoisomer;toposelective synthesis
摘要：
Six topoisomers consisting of diethoxycarbonyl glycoluril have been successfully synthesized in one-pot by using a “figure-of-seven” building block through anti-connectivity and syn-connectivity reactions, respectively. The structures of all six topoisomers were first determined by X-ray crystallography. The finding that (±) CT isomers are the dominant products under thermodynamic control can be explained by the calculated relative energies of the six topoisomers. That the (±) CT isomers have the lowest energy is most likely due to the additional intramolecular electrostatic interactions between-NO2 and-OMe groups. The biological activities of the topoisomers were primitively investigated and the results of bioassay showed that the six topoisomers possessed obvious difference of herbicidal activity.
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1,2-Dibromo-4,5-bis(bromomethyl)benzene
作者：
She, Neng-Fang
（ ;Zhao, Qin;Yin, Guo-Dong;Wu, An-Xin
* （ 期刊：
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY ,2006年62(6):o2523-o2524 ISSN：2053-2296
作者机构：
[She, Neng-Fang; Wu, An-Xin; Zhao, Qin; Yin, Guo-Dong] Cent China Normal Univ, Coll Chem, Key Lab Pesticides & Chem Biol, Minist Educ, Wuhan 430079, Peoples R China.
通讯机构：
[Wu, An-Xin] C;Cent China Normal Univ, Coll Chem, Key Lab Pesticides & Chem Biol, Minist Educ, Wuhan 430079, Peoples R China.
摘要：
In the crystal structure of the title compound, C8H 6Br4, the packing of the molecules is mainly governed by an intermolecular π-π interaction. © 2006 International Union of Crystallography. All rights reserved.
语种：
英文
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Diethyl 2,3-bis(4-methoxybenzoyl)succinate
作者：
Liu, HX;Wang, ZG
* ;Wu, AX
（ 期刊：
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY ,2006年62(4):o1284-o1285 ISSN：2053-2296
通讯作者：
Wang, ZG
作者机构：
[Wang, ZG] Cent China Normal Univ, Coll Chem, Minist Educ, Key Lab Pesticides & Chem Biol, Wuhan 430079, Peoples R China.;Hubei Inst Nationalities, Sch Chem & Environm Engn, Enshi 445000, Hubei, Peoples R China.
通讯机构：
[Wang, ZG] C;Cent China Normal Univ, Coll Chem, Minist Educ, Key Lab Pesticides & Chem Biol, Wuhan 430079, Peoples R China.
摘要：
The title molecule, C24H26O8, has approximate twofold rotation symmetry and the crystal structure is stabilized by intermolecular C-H⋯π interactions. © 2006 International Union of Crystallography All rights reserved.
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Diethyl 5,10-dihydro-6-iodo-4,11-dioxo-cis-1H,3H,4H,11H-2-oxa-3a,4a,10a, 11a-tetraazabenz[f]indeno[2,1,7-ija]azulene-11b,11c-dicarboxylate
作者：
Chen, Yun-Feng
* ;Xu, Mei;Wu, An-Xin
（ 期刊：
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY ,2006年62(6):o2254-o2255 ISSN：2053-2296
通讯作者：
Chen, Yun-Feng
作者机构：
[Wu, An-Xin; Xu, Mei; Chen, Yun-Feng; Chen, YF] Cent China Normal Univ, Coll Chem, Minist Educ, Key Lab Pesticides & Chem Biol, Wuhan 430079, Peoples R China.
通讯机构：
[Chen, Yun-Feng] C;Cent China Normal Univ, Coll Chem, Minist Educ, Key Lab Pesticides & Chem Biol, Wuhan 430079, Peoples R China.
摘要：
The title compound, C20H21IN4O 7, is a glycoluril derivative which contains five fused rings. An iodobenzene ring is fused to a seven-membered ring linked to two of the N atoms from the separate rings of the glycoluril system, and the other two N atoms are linked to an O atom by two of the methylene groups. The structure of the compound possesses normal geometrical parameters. The crystal packing is consolidated by intermolecular hydrogen bonds, resulting in a two-dimensional network. © 2006 International Union of Crystallography. All rights reserved.
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Synthesis of novel molecular clips based on diethoxycarbonyl glycoluril
作者：
Yin, GD
* ;Wang, ZG;Chen, YF;Wu, AX
（ ;Pan, YJ
期刊：
SYNLETT ,2006年2006(1):49-52 ISSN：0936-5214
通讯作者：
Yin, GD
作者机构：
[Yin, GD] Cent China Normal Univ, Key Lab Pesticide & Chem Biol, Minist Educ, Wuhan 430079, Peoples R China.;Zhejiang Univ, Dept Chem, Hangzhou 310027, Peoples R China.
通讯机构：
[Yin, GD] C;Cent China Normal Univ, Key Lab Pesticide & Chem Biol, Minist Educ, Wuhan 430079, Peoples R China.
关键词：
molecular clips;diethoxycarbonyl glycoluril;aromatic amines;synthetic receptors;conformers
摘要：
A novel class of molecular clips was synthesized, which are soluble in most non-polar organic solvents. Aromatic amines and diethoxycarbonyl glycoluril were used for the first time in this type of reaction. All reaction products gave satisfying 1H NMR, 13C NMR, MS, and IR spectra. In addition, the structure and conformation of 4d were confirmed by single crystal X-ray diffraction. © Georg Thieme Verlag Stuttgart.
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6,9-Dibromo-2a,10b-diphenyl-2a,5,10,10b-tetrahydro-2H,3H-2,3,4a, 10a-tetraazabenzo[g]cyclopenta[cd]azulene-1,4-dione monohydrate
作者：
She, Neng‐Fang
（ ;Hu, Sheng‐Li;Guo, Hui‐Zhen;Wu, An‐Xin
（ 期刊：
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY ,2006年62(5):o1754-o1755 ISSN：2053-2296
通讯作者：
Wu, AX
作者机构：
[She, Neng‐Fang; Wu, An‐Xin; Guo, Hui‐Zhen; Hu, Sheng‐Li] Cent China Normal Univ, Coll Chem, Key Lab Pesticides & Chem Biol, Minist Educ, Wuhan 430079, Peoples R China.
通讯机构：
[Wu, AX] C;Cent China Normal Univ, Coll Chem, Key Lab Pesticides & Chem Biol, Minist Educ, Wuhan 430079, Peoples R China.
摘要：
The title compound, C24H18Br2N 4O2·H2O, forms a supramolecular structure via N - H⋯O, O - H⋯O and C - H⋯O hydrogen bonds. In the crystal structure, the water molecule serves as a bifurcated hydrogen-bond acceptor and as a hydrogen-bond donor. © 2006 International Union of Crystallography. All rights reserved.
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(2R,3S)-diethyl 2,3-dibenzoylsuccinate
作者：
Hu, SL;Liu, XM;Guo, HZ;Wu, AX
* （ 期刊：
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY ,2006年62(5):o1966-o1967 ISSN：2053-2296
作者机构：
[Wu, AX] Cent China Normal Univ, Minist Educ, Key Lab Pesticides & Chem Biol, Coll Chem, Wuhan 430079, Peoples R China.;Hubei Normal Univ, Dept Chem & Environm Engn, Huangshi 435002, Peoples R China.
通讯机构：
[Wu, AX] C;Cent China Normal Univ, Minist Educ, Key Lab Pesticides & Chem Biol, Coll Chem, Wuhan 430079, Peoples R China.
摘要：
In the crystal structure of the title compound, C22H 22O6, the asymmetric unit consists of one half-molecule with the other half generated by a centre of inversion. The crystal packing is stabilized by C - H⋯O intermolecular interactions. © 2006 International Union of Crystallography. All rights reserved.
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Efficient C-C double-bond formation reaction via a new synthetic strategy: A self-sorting tandem reaction
作者：
Yin, Guodong;Zhou, Baohan;Meng, Xianggao;Wu, Anxin
* （ ;Pan, Yuanjiang
期刊：
Organic Letters ,2006年8(11):2245-2248 ISSN：1523-7060
作者机构：
Cent China Normal Univ, Key Lab Pesticide & Chem Biol, Minist Educ, Wuhan 430079, Peoples R China.;Zhejiang Univ, Dept Chem, Hangzhou 310027, Peoples R China.;[Wu, Anxin] Cent China Normal Univ, Key Lab Pesticide & Chem Biol, Minist Educ, 152 Luoyu Rd, Wuhan 430079, Peoples R China.
通讯机构：
[Wu, Anxin] C;Cent China Normal Univ, Key Lab Pesticide & Chem Biol, Minist Educ, 152 Luoyu Rd, Wuhan 430079, Peoples R China.
摘要：
A novel and efficient carbon-carbon double-bond formation reaction via coupling of aryl or heteroaryl methyl ketones has been developed. A dimethyl sulfoxide-iodine-CuO system was proven to be efficient for this reaction and afforded the expected products in good yields. A new synthetic strategy, a self-sorting tandem reaction, was involved in this type of reaction and was presented for the first time. © 2006 American Chemical Society.
语种：
英文
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One-pot synthesis of novel molecular clips and macrocyclic polyamines derived from bis(ethoxycarbonyl)glycoluril
作者：
Li, Yitao;Yin, Guodong;Guo, Huizhen;Zhou, Baohan;Wu, Anxin
* （ 期刊：
SYNTHESIS-STUTTGART ,2006年2006(17):2897-2902 ISSN：0039-7881
作者机构：
[Wu, Anxin; Li, Yitao; Yin, Guodong; Guo, Huizhen; Zhou, Baohan] Cent China Normal Univ, Minist Educ, Key Lab Pesticide & Chem Biol, Wuhan 430079, Peoples R China.
通讯机构：
[Wu, Anxin] C;Cent China Normal Univ, Minist Educ, Key Lab Pesticide & Chem Biol, Wuhan 430079, Peoples R China.
关键词：
amines;polyamines;macrocycles;molecular clips;glycoluril
摘要：
A new class of molecular clips and two novel macrocyclic polyamines were synthesized in one-pot procedures from aliphatic amines, formaldehyde, and rigid bis(ethoxycarbonyl)glycoluril. Apart from characterization of all reaction products by <sup>1</sup>H NMR, <sup>13</sup>C NMR, mass, and IR spectroscopy, a clip molecule and two macrocyclic cycloadducts were also studied by X-ray crystallography. ©Georg Thieme Verlag Stuttgart.
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Substituent effects control the self-association of molecular clips in the crystalline state
作者：
Wang, Zhi-Guo;Zhou, Bao-Han;Chen, Yun-Feng;Yin, Guo-Dong;Li, Yi-Tao;...
期刊：
JOURNAL OF ORGANIC CHEMISTRY ,2006年71(12):4502-4508 ISSN：0022-3263
作者机构：
[Wu, An-Xin] Cent China Normal Univ, Coll Chem, Minist Educ, Key Lab Pesticide & Chem Biol, Wuhan 430079, Peoples R China.;Univ Maryland, Dept Chem & Biochem, College Pk, MD 20742 USA.
通讯机构：
[Wu, An-Xin] C;Cent China Normal Univ, Coll Chem, Minist Educ, Key Lab Pesticide & Chem Biol, Wuhan 430079, Peoples R China.
摘要：
We report the X-ray crystal structure of 11 molecular clips and analyze the influence of substituents ( e. g., OMe, Me, and NO2) and their location on the observed crystal packing. Molecular clips 3a and 3b form tapelike structures in the crystal due to pi-pi interactions between the aromatic walls. Compounds 3d, 3eC, and 3fC form dimers driven by critical C-H center dot center dot center dot O interactions and then form tapes driven by pi-pi interactions in the crystal. These two building motifs, pi-pi and C-H center dot center dot center dot O interactions, can be used to rationalize the enantio- and diastereoselectivity observed in the X-ray crystal structures of the remaining five molecular clips. For example, the C-H center dot center dot center dot O interactions are found to dictate the formation of homochiral dimers in the structures of (+/-)-3eT and (+/-)-3fT and to control the diastereoselective formation of 6a(2)-6c(2) dimeric motifs with internal p-dimethoxy-o-xylylene walls. Overall, the results suggest that substituent effects that induce even weak intermolecular interactions ( e. g., C-H center dot center dot center dot O) can be used to reliably control crystal packing within glycoluril-based systems.
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英文
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The absolute configuration of a nitroxide spin labeled derivative of podophyllotoxin determined by the crystal structure
作者：
Zhou, Baohan;Yin, Guodong;Meng, Xianggao;Li, Yitao;Wu, Anxin
* （ 期刊：
CANADIAN JOURNAL OF CHEMISTRY ,2006年84(12):1603-1606 ISSN：0008-4042
作者机构：
[Wu, Anxin; Meng, Xianggao; Li, Yitao; Yin, Guodong; Zhou, Baohan] Cent China Normal Univ, Coll Chem, Minist Educ, Lab Pesticide & Chem Biol, Wuhan 430079, Peoples R China.
通讯机构：
[Wu, Anxin] C;Cent China Normal Univ, Coll Chem, Minist Educ, Lab Pesticide & Chem Biol, Wuhan 430079, Peoples R China.
关键词：
Crystal structure;Nitroxyl radical;Podophyllotoxin;Synthesis
摘要：
The crystal structure of the nitroxide spin labeled derivative of podophyllotoxin was first reported. X-ray analysis demonstrated that four contiguous chiral centers in the molecule, C1, C2, C3, and C4, adopt cis- (1:2), trans-(2:3), and cis- (3:4) arrangement. ©2006 NRC.
语种：
英文
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Diethyl 2-(1,3-benzodioxol-5-yl)-5-(3,4-dimethoxy-phenyl)furan-3,4- dicarboxylate
作者：
Hu, SL;Wang, ZG;Wu, AX
* （ 期刊：
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY ,2005年61(9):o2801-o2803 ISSN：2053-2296
作者机构：
[Wu, AX] Cent China Normal Univ, Coll Chem, Minist Educ, Key Lab Pesticides & Chem Biol, Wuhan 430079, Peoples R China.;Hubei Normal Univ, Dept Environm Chem & Engn, Huangshi 435002, Peoples R China.
通讯机构：
[Wu, AX] C;Cent China Normal Univ, Coll Chem, Minist Educ, Key Lab Pesticides & Chem Biol, Wuhan 430079, Peoples R China.
摘要：
In the title compound, C25H24O9, the substituted benzene rings are twisted away from the furan ring. The dihedral angle between the two benzene rings is 52.1 (1)°. In the crystal structure, the molecules exist as hydrogen-bonded dimers, the molecules being connected through very weak C-H⋯O hydrogen bonds. © 2005 International Union of Crystallography Printed in Great Britain - all rights reserved.
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Diethyl 4,8-dioxo-2,6-di-p-chlorophenyl-1,3,5,7-tetrahydro-2,3a,4a,6,7a,8a- hexaazacyclopenta-[def]fluorene-8b,8c-dicarboxylate
作者：
Yin, GD;Zhou, BH;Wu, AX
* （ 期刊：
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY ,2005年61(9):o2787-o2788 ISSN：2053-2296
作者机构：
[Wu, AX; Yin, GD; Zhou, BH] Cent China Normal Univ, Coll Chem, Key Lab Pesticide Chem Biol, Minist Educ, Wuhan 430079, Peoples R China.
通讯机构：
[Wu, AX] C;Cent China Normal Univ, Coll Chem, Key Lab Pesticide Chem Biol, Minist Educ, Wuhan 430079, Peoples R China.
摘要：
In the title compound, C28H32Cl2N 6O6, the dihedral angle between the two adjacent five-membered rings in the glycoluril unit is 70.18 (9)° and molecules are connected mainly by G-H⋯O intermolecular interactions. © 2005 International Union of Crystallography Printed in Great Britain - all rights reserved.
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2,6-Dibenzyl-8b,8c-diphenyl-2,3a,4a,6,7a,8a-hexaazaperhydrocyclopenta[def] fluorene-4,8-dione
作者：
Li, Yi‐Tao;Long, Tao;Wu, An‐Xin
（ 期刊：
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY ,2005年61(8):o2374-o2375 ISSN：2053-2296
通讯作者：
Wu, AX
作者机构：
[Wu, An‐Xin; Li, Yi‐Tao; Long, Tao] Cent China Normal Univ, Coll Chem, Minist Educ, Key Lab Pesticide & Chem Biol, Wuhan 430079, Peoples R China.
通讯机构：
[Wu, AX] C;Cent China Normal Univ, Coll Chem, Minist Educ, Key Lab Pesticide & Chem Biol, Wuhan 430079, Peoples R China.
摘要：
The molecule of the title compound, C34H32N 6O2, exhibits normal geometric parameters. The two terminal phenyl rings make a dihedral angle of 69.24 (2)° with each other. The crystal packing is stabilized mainly by van der Waals interactions. © 2005 International Union of Crystallography Printed in Great Britain - all rights reserved.
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Tetraethyl 2,2′-(p-phenylenedimethylene)dimalonate
作者：
Chen, AH;Wang, ZG;Yin, GD;Wu, AX
* （ 期刊：
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY ,2005年61(10):o3240-o3241 ISSN：2053-2296
作者机构：
[Wu, AX; Wang, ZG; Yin, GD; Chen, AH] Cent China Normal Univ, Coll Chem, Minist Educ, Key Lab Pesticides & Chem Biol, Wuhan 430079, Peoples R China.
通讯机构：
[Wu, AX] C;Cent China Normal Univ, Coll Chem, Minist Educ, Key Lab Pesticides & Chem Biol, Wuhan 430079, Peoples R China.
摘要：
The molecule of the title compound, C22H30O8, contains a crystallographic inversion centre located at the middle of the benzene ring.
语种：
英文
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rac-Diethyl 2,3-bis(2-methoxybenzoyl)succinate
作者：
Meng, Xiang‐Gao;Wu, An‐Xin
（ 期刊：
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY ,2005年61(10):o3203-o3204 ISSN：2053-2296
通讯作者：
Meng, XG
作者机构：
[Wu, An‐Xin; Meng, Xiang‐Gao] Cent China Normal Univ, Dept Chem, Wuhan 430079, Peoples R China.
通讯机构：
[Meng, XG] C;Cent China Normal Univ, Dept Chem, Wuhan 430079, Peoples R China.
摘要：
In the rac isomer mixture of the title compound, C24H 26O8, the molecules are weakly linked via C-H⋯O and π-π interactions, forming a three-dimensional network. © 2005 International Union of Crystallography Printed in Great Britain - all rights reserved.
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1,3:4,6-Bis(1,4-diphenylethynyl-2,3-xylylene)tetrahydro-3a, 6a-bis(ethoxycarbonyl)imidazo[4,5-d]-imidazole-2,5(1H,3H)-dione, a molecular clip based on di(ethoxycarbonyl)glycoluril
作者：
She, Neng‐Fang
（ ;Guo, Hui‐Zhen;Wu, An‐Xin
（ 期刊：
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY ,2005年61(7):o2003-o2004 ISSN：2053-2296
通讯作者：
Wu, AX
作者机构：
[She, Neng‐Fang; Wu, An‐Xin; Guo, Hui‐Zhen] Cent China Normal Univ, Key Lab Pesticide & Chem Biol, Minist Educ, Coll Chem, Wuhan 430079, Peoples R China.
通讯机构：
[Wu, AX] C;Cent China Normal Univ, Key Lab Pesticide & Chem Biol, Minist Educ, Coll Chem, Wuhan 430079, Peoples R China.
摘要：
The molecule of the title compound, C58H42N 4O6, a molecular clip based on the glycoluril framework, occupies a special position on a twofold axis passing through the mid-point of the gycoluril C-C bond. The planes of the central benzene rings in the opposite wings of the molecular clip form a dihedral angle of 41.6 (4)°. No dimers typical for molecular clip packings are observed in the crystal structure of the title compound. © 2005 International Union of Crystallography Printed in Great Britain - all rights reserved.
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2,2,6,6-Tetramethylpiperidin-4-ol
作者：
She, NF
（ ;Guo, HZ;Yin, GD;Wu, AX
* （ 期刊：
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY ,2005年61(9):o2902-o2903 ISSN：2053-2296
作者机构：
[She, NF; Wu, AX; Guo, HZ; Yin, GD] Cent China Normal Univ, Coll Chem, Key Lab Pesticides & Chem Biol, Minist Educ, Wuhan 430079, Peoples R China.
通讯机构：
[Wu, AX] C;Cent China Normal Univ, Coll Chem, Key Lab Pesticides & Chem Biol, Minist Educ, Wuhan 430079, Peoples R China.
摘要：
The molecule of the title compound, C9H19NO, lies on a mirror plane. Intermolecular N - H⋯O and O - H⋯N hydrogen bonds are observed in the crystal structure. © 2005 International Union of Crystallography Printed in Great Britain - all rights reserved.
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